By Annie Davis
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With this nebulizer, more analyte can be transported into the plasma at a lower nebulizer gas flow rate than that seen with pneumatic nebulizers. This increases the sensitivity and improves detection limits since samples have a longer residence time in the plasma. However, the high Atomic Emission, Methods and Instrumentation 75 Figure 7 Ultrasonic nebulizer schematic. Reprint permission from Ingle JD and Crouch SR (1988) Spectrochemical Analysis. Englewood Cliffs, NJ: Prentice Hall. efficiency also allows more water to enter the plasma, producing a cooling effect, which may decrease analyte ionization.
Additionally, samples with high salt content and limited volume can be analyzed with electrothermal vaporization. Figure 8 furnace. Illustration of electrothermal vaporization graphite by presenting the sample in a gaseous form to the plasma. Introducing the analyte in a gaseous form eliminates the use of a nebulizer and a spray chamber. It also provides nearly 100% analyte transport efficiency, which subsequently improves the detection limits. Additional benefits include no blockage problems, the possibility of matrix separation and analyte preconcentration, and the absence of water, which reduces the levels of many polyatomic ion species.
IOWA: Ames Laboratory, US Department of Energy. Ingle JD and Crouch SR (1988) Spectrochemical Analysis. Englewood Cliffs, NJ: Prentice-Hall. ) (1992) Inductively Coupled Plasmas in Analytical Atomic Spectrometry. Weinheim: VCH. Slickers K (1993) Automatic Atomic Emission Spectroscopy. Giessen: Bru¨hlsche Universita¨tsdruckerei. ) (1990) Sample Introduction in Atomic Spectroscopy, Analytical Spectroscopy Library No. 4. Amsterdam: Elsevier. ) (1994) Charge-Transfer Devices in Spectroscopy. Weinheim: VCH.
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